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Beilstein J. Org. Chem. 2018, 14, 11–24, doi:10.3762/bjoc.14.2
Graphical Abstract
Figure 1: The three major methods for the synthesis of GAuNPs. (a) Direct reduction of an Au3+ salt in the pr...
Scheme 1: The non-catalysed azide–alkyne Huisgen cycloaddition (NCAAC) between an organic azide (1,3-dipole) ...
Scheme 2: Ligand exchange and NCAAC on an AuNP surface. Reagents and conditions: (a) Br(CH2)11SH in DCM, 60 h...
Scheme 3: Azide functionalization and NCAAC on an AuNP surface using electron deficient alkynes. Reagents and...
Scheme 4: NCAAC performed under hyperbaric conditions. Reagents and conditions: (a) Br(CH2)11SH in C6H6, 48 h...
Scheme 5: The synthesis of AuNPs functionalized with strained alkyne derivatives. HBTU = O-benzotriazole-N,N,N...
Scheme 6: A schematic representation of the SPAAC between azide-functionalized polymersomes and strained alky...
Scheme 7: Functionalization of AuNPs with an azide containing thiol ligand, and subsequent attachment to an a...
Scheme 8: Surface modification of AuNPs using microwave-assisted CuAAC. Reagents and conditions: (a) HS(CH2)11...
Scheme 9: AuNP functionalization and efficient CuAAC with a range of alkynes reported by Boisselier et al. [62]. ...
Scheme 10: Schematic illustration of: (a) AuNP deposition on a carbon electrode; (b) formation of alkyne-termi...
Scheme 11: (a) Synthesis of the alkyne-terminated thiol (ATT) ligand 33; (b) synthesis of 12 nm sized ATT-AuNP...
Scheme 12: Synthesis of (a) cyclooctyne-functionalized AuNPs and (b) GAuNPs using SPAAC [82].